Formules Courtes - addiactive · Les « Formules courtes » de ce dossier spécial sont ... imparts intense moisturization to thirsty and dry ... After the polymer has thoroughly

Dossier spécial

Ce dossier spécial « Formules courtes » regroupe des idées de formules réalisées avec moins de 10 ingrédients ! Ces bases simples et sans ingrédient superflu permettront de nourrir vos projets dans différents univers :

> Dermo-cosmétique > Peaux fragiles et sensibles > Cible bébé et enfants > Formules économiques réalisées dans un esprit « Formuler malin ou comment faire mieux avec moins ?! »

Formules CourtesFormules CourtesFormules Courtes

Les « Formules courtes » de ce dossier spécial sont réalisées avec moins de 10 ingrédients. NB : Elles ne sont plus toujours échantillonables

Ces bases simples et sans ingrédient superflu sont formulées à partir de différents systèmes émulsionnants. Elles entreront dans différentes gammes (formules simples / formules simples naturelles / formules bébé et enfants / soins spécifiques).

Dossier «Dossier «Dossier « Formules CourtesFormules CourtesFormules Courtes »»»

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Formules simplesAnti-imperfection Cream 1377_1_01 ● p.4Japanese Serum 1400_2_02 ● p.5Rapid Results Skin Quenching Cream B-0073 (EU) ● p.6Refined Simplicity JB 2412 ● p.721st Century Hydrating Cream F-0047 ● p.9After Shave Balm for Sensitive Skin M-0006 ● p.10

Formules simples naturellesCreamy Emulsion 1238_2_01 ● p.12Naked Cream Gel 1305_1_09 ● p.13Delight and Nourrish1356_1_11 ● p.14Soothing Day Cream JB 2730_A ● p.15

Formules bébé & enfantEdible Mum and Baby Balm 1304_1_01 p.17Moisturizing Baby Cream JB 2806-K ● ● p.18W/O Baby Cream MM 7516 ● p.19Mommy ’n’ Me Sprayable Liquid Powder O-0005 (EU) ● p.20PEG-Free Emulsion for Baby Wipe W-0001 (EU) ● p.21

Soins spécifiquesCloud Mask JB 2840_H ● p.23Translucent SkinTonerO-0050B (AP) ● p.24

Cliquez sur le nom de la formule pour atteindre la page correspond ante

FormulesFormulesFormulessimplessimplessimples

ANTI-IMPERFECTION CREAM

1377-1.01

This formula is presented in good faith, however, no warranty as to the accuracy or completeness of results, or fitness for a particular use is given, nor is freedom from the infringement of any intellectual/industrial property rights to be inferred.

It is provided "as is" for your consideration, investigation and verification. To the extent permissible by applicable law, Gattefossé shall in no way be liable for any reliance upon information or materials provided.

Phase Material Name INCI Supplier Properties % Material

A EMULIUM

® DELTA

CETYL ALCOHOL, GLYCERYL STEARATE, PEG-75 STEARATE, CETETH-20,

STEARETH-20

GATTEFOSSE O/W

emulsifier 3,0

CETIOL CC DICAPRYLYL CARBONATE BASF emollient 3,0

CETIOL C5 COCO-CAPRYLATE BASF emollient 4,0

B DEMINERALIZED WATER WATER - - 80,6

CARBOPOL ULTREZ 20 ACRYLATES/C10-30 ALKYL ACRYLATE CROSSPOLYMER

LUBRIZOL gelling agent 0,2

GLYCERIN GLYCERIN - moisturizing agent

3,0

SATIAXANE CX91 XANTHAN GUM CARGILL gelling agent 0,2

C SODIUM HYDROXIDE (10 % SOL.) WATER, SODIUM HYDROXIDE - base 0,4

D PRESERVATIVE PRESERVATIVE - preservative 0,4

E CYTOBIOL

TM IRIS A 2

PROPANEDIOL, WATER, ALCOHOL, IRIS FLORENTINA ROOT EXTRACT, ZINC

SULFATE, RETINYL PALMITATE

GATTEFOSSE anti-acne, sebum

control 5,0

F PERFUME PRECIEUSE 0601579 PARFUM EXPRESSIONS PARFUMEES

perfume 0,2

100,0

Operating Instructions

- Sprinkle Carbopol Ultrez 20 over water, leave to hydrate. - Disperse Satiaxane CX91 (10 min.) into B. - Unter mixing, add A heated to 75°C to B heated to 75°C. - Add C and D. - Add E about 35 °C then F. - Cool under mixing.

Trial Notes

- Aspect : white cream - pH : 5.3 ± 0.5 - Viscosity (spindle B,speed 5) : 50 000 mPa.s after 24H.

JAPANESE SERUM

1400-2.02




A DEMINERALIZED WATER WATER - - 83,25

CARBOPOL ULTREZ 21 ACRYLATES/C10-30 ALKYL ACRYLATE CROSSPOLYMER

LUBRIZOL gelling agent 0,10


3,00

BUTYLENE GLYCOL BUTYLENE GLYCOL - dispersing agent, solubilizer

5,00


B EMULIUM

® MELLIFERA

POLYGLYCERYL-6 DISTEARATE, JOJOBA ESTERS, POLYGLYCERYL-3

BEESWAX, CETYL ALCOHOL

GATTEFOSSE O/W emulsifier 3,00

PRESERVATIVE PRESERVATIVE - preservative 1,00

C KF-96-6CS DIMETHICONE SHINETSU feeling agent 4,00

D SODIUM HYDROXIDE (10 % SOL.) WATER, SODIUM HYDROXIDE - base 0,25

E PERFUME SOINS PRESTIGE ARX/34516

PARFUM AROMAX perfume 0,20

100,00


- Sprinkle Carbopol Ultrez 21 over water, leave to hydrate. - Under mxing, add glycerin, butylene glycol and Satiaxane CX 91, then heat to 75°C. - Heat B to 75°C. - Under rapid mixing (rotor/stator 2000 rpm) add B to A. - Maintain this rapid mixing for about 5 min. - Add phase C, continue rapid mixing for about 5 min. - Add phase D, continue rapid mixing for about 5 min. - Cool under moderate mixing and at about 35°C, add E.

Trial Notes

- Aspect : White Serum - pH = 6.0 ± 0.5 - Viscosity Brookfield RV (spindle A, speed 5) : approx. 7 000 mPa.s after 24H

:

This cream, enriched with hydrating actives, imparts intense moisturization to thirsty and dry skin. The high electrolyte dead sea salt extract is stabilized by the synergy between Novemer™* EC-2 and Carbopol®* Ultrez 20 Polymers, providing viscosity and excellent emulsion stabilization in this cushiony cream. Schercemol™* NGDO Ester offers additional emolliency and softness, leaving the skin supple and smooth.

Rapid Results Skin Quenching Cream

INCI Name, Trade Name Weight % Function

A. 1. Deionized Water 54.40 Diluent

2. Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Carbopol®* Ultrez 20 Polymer

0.40 Rheology Modifier

3. Sodium Acrylates/Beheneth-25 Methacrylate Crosspolymer (and) Hydrogenated Polydecene (and) Lauryl Glucoside, Novemer™* EC-2 Polymer (20 %TS)

5.00 Rheology Modifier / Emulsion Stabilizer

4. Neopentyl Glycol Diethylhexanoate, Schercemol™* NGDO Ester

10.00 Emollient

5. Onopordum Acanthium Flower/Leaf/Stem Extract (and) Alcohol (and) Water, Gatuline® Skin-Repair BIO

2.00 Botanical Extract

6. Phenoxyethanol (and) Ethylhexylglycerin, Euxyl® PE 9010

1.00 Preservative

7. Fragrance, Creamans

0.10 Fragrance

B. 8. Deionized Water 25.00 Diluent

9. Sea Salt, Dead Sea Salt (Ground)

1.00 Skin Conditioner

10. Sodium Hydroxide (18%) 1.10 Neutralizer

Product Properties: Appearance White-yellow cream

pH 6.0 – 6.5

Viscosity (mPa·s)** 11,000 – 16,000

Stability: Passed 3 months @ 25 °C and 45 °C, Passed 5 freeze/thaw cycles Novemer™* EC-2 Polymer (%TS) 1.0 Recommended Packaging Jar **Brookfield RV, DVII+ Viscometer spindle #5 @ 20 rpm, 25 °C @ 24 hours

B-0073(EU)

The information contained herein is believed to be reliable, but no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for particular applications or the results to be obtained. The information often is based on laboratory work with small-scale equipment and does not necessarily indicate end product performance or reproducibility. Formulations presented may not have been tested for stability and should be used only as a suggested starting point. Because of the variations in methods, conditions and equipment used commercially in processing these materials, no warranties or guarantees are made as to the suitability of the products for the applications disclosed. Full-scale testing and end product performance are the responsibility of the user. Lubrizol Advanced Materials, Inc. shall not be liable for and the customer assumes all risk and liability for any use or handling of any material beyond Lubrizol Advanced Materials, Inc.’s direct control. The SELLER MAKES NO WARRANTIES, EXPRESS OR IMPLIED, INCLUDING, BUT NOT LIMITED TO, THE IMPLIED WARRANTIES OF MERCHANTABILITY AND FITNESS FOR A PARTICULAR PURPOSE. Nothing contained herein is to be considered as permission, recommendation, nor as an inducement to practice any patented invention without permission of the patent owner.

Lubrizol Advanced Materials, Inc. is a wholly owned subsidiary of The Lubrizol Corporation Noveon is a registered trademark of The Lubrizol Corporation *Trademark owned by The Lubrizol Corporation © Copyright 2012 Lubrizol Advanced Materials, Inc.

Supplier References: Lubrizol Advanced Materials, Inc. (Noveon®* Consumer Specialties) (2, 3, 4)

Gattefossé (5)

Schülke & Mayr (6)

Essential Compositions (7)

A & E Connock (9)

VWR (10)

B-0073(EU)

Edition: February 10, 2012

Reference #: LLN-037-11 (111013-01) (LUBQ)

Original Edition: January 17, 2012

North America 9911 Brecksville Road

Cleveland, OH 44141-3247 TEL: 216.447.5000 TEL: 800.379.5389 FAX: 216.447.5250

Mexico Avenida Interceptor Pte. #69 Parque Industrial ‘La Joya’

Cuautitlán, Izcalli - Mexico City Edo. de México 54730, México

TEL: 52.55.3067.0860 FAX: 52.55.5870.8956

Brazil Av. Fagundes Filho

134 - Cj. 101, 10th floor Edificio Victoria Office Center

São Judas, 04304-010 São Paulo TEL: 55.11.4082.1330 FAX: 55.11.4082.1345

Europe, Middle East and Africa

Chaussée de Wavre, 1945 B-1160 Brussels, Belgium

TEL: 32.2.678.19.11 FAX: 32.2.678.20.02

Asia Pacific 1107-1110 Shui On Centre

6-8 Harbour Road Wanchai, Hong Kong TEL: 852.2508.1021 FAX: 852.2512.2241

South Asia 501 & 501A, Omega

Hiranandani Business Park Powai

Mumbai 400 076 India TEL: 91.22.6698.0590 / 91

FAX: 91.22.6602.7888

China 27/F Majesty Building

No. 138 Pudong Avenue Shanghai 200120, PRC TEL: 86.21.3866.0366 FAX: 86.21.5887.6981

For more information visit www.personalcare.noveon.com or contact your nearest Lubrizol Advanced Materials location.

Procedure:

1. PART A: Sprinkle Carbopol®* Ultrez 20 Polymer on the surface of Deionized Water. After the polymer has thoroughly wet-out, mix at low speed.

2. Add Novemer™* EC-2 Polymer and mix until uniform.

3. Add Schercemol™* NGDO Ester and mix with vigorous agitation. Mix until uniform.

4. Add the remaining PART A ingredients and mix until uniform.

5. PART B: In a separate vessel, mix PART B ingredients until uniform.

6. Slowly add PART B to PART A with rapid mixing. Mix until uniform.

REFINED SIMPLICITY JB 2412

This formula is presented in good faith, and we believe it is correct, but no warranty as to accuracy of results, or fitness for a particular use is given, nor is freedom from patent infringement to be inferred. It is offered solely for your consideration, investigation and verification.

Cette formule correspond à notre meilleure connaissance et est fournie à titre indicatif. Elle n'implique aucune garantie de notre part en ce qui concerne l'emploi et les méthodes d'emploi de ladite formule et de ses ingrédients, ceci étant de la seule responsabilité des utilisateurs, qui devront en particulier vérifier qu'ils ne contreviennent pas à des brevets existants.

©Copyright GATTEFOSSÉ

Ingredients INCI designation % W/W Ingredient Function

Phase 1EMULIUM® 22 (1) TRIBEHENIN PEG-20 ESTERS 4.00 Emulsifier o/wLABRAFAC CC (1) CAPRYLIC/CAPRIC TRIGLYCERIDE 15.00 Emollient

Phase 2DEMINERALIZED WATER WATER 78.95CARBOPOL ULTREZ 10 (2) CARBOMER 0.25 Gelling agentRHODICARE S (3) XANTHAN GUM 0.20 Gelling agent

Phase 3SODIUM HYDROXIDE (10 % SOL.) SODIUM HYDROXIDE 0.50 Neutralizing agent

Phase 4PERFUME FRAIS 4164 (4) 0.10 PerfumePRESERVATIVE 1.00 Preservative

100,00(1) GATTEFOSSE SAS / (2) LUBRIZOL / (3) RHODIA / (4) M.L.W

APPAREANCE: White supple cream

MANUFACTURING PROCESS: - Sprinkle Carbopol Ultrez 10 over water, leave to stand.- Under mixing, add Rhodicare S to II.- Heat I and II to 75°C.- Under rapid mixing (Rotor/Stator 2000 rpm), add I to II.- Maintain rapid mixing for about 5 min then add III.- Continue rapid mixing for about 5 min.- Cool under planetary stirring and at about 35°C, add IV .- Complete cooling.

PROPERTIES: - pH = 5.5 ± 0.5- Viscosity Brookfield RV (spindle B, speed 5): approx. 21 000 mPa.s after 24 h.

ASPECT: Crème souple blanche

MODE OPERATOIRE: - Saupoudrer Carbopol Ultrez 10 dans l'eau, laisser s'hydrater- Sous agitation, ajouter Rhodicare S à II.- Chauffer les phases I et II à 75 °C.- Sous agitation rapide (Rotor/Stator 2000 tr/min ), ajouter I dans II. - Maintenir l'agitation rapide pendant environ 5 min. - Ajouter III.- Poursuivre l'agitation rapide pendant environ 5 min- Refroidir sous agitation planétaire et vers 35°C ajouter IV.- Terminer le refroidissement.

REFINED SIMPLICITY JB 2412




PROPRIÉTÉS: - pH = 5,5 ± 0,5- Viscosité Brookfield RV (mobile B, vitesse 5): environ 21 000 mPa.s après 24 h.

:

In the 21st century, time is money and sensory is a priority. This cream can be prepared in less than 5 minutes. It is simple, cost-effective, stable, and beautiful. Novemer™* EC-2 Polymer is used as the primary emulsifier, thickener, and stabilizer in this pH 5.5 emulsion. It is also an efficient rheology and sensory modifier in this high electrolyte formula. Schercemol™* CO Ester creates a pleasant glide between fingers and onto body without oily residue or afterfeel. Schercemol™* NGDC Ester leaves skin feeling silky smooth.

21st Century Hydrating Cream



2. Lactic Acid (90%), HiPure 90

0.35 pH Adjuster

3. Glycerin, Glycerin, 99.6% USP

3.00 Humectant

B. 4. DMDM Hydantoin (and) Iodopropynyl Butylcarbamate, Glydant® Plus Liquid

0.40 Preservative

C. 5. Sodium Acrylates/Beheneth-25 Methacrylate Crosspolymer (and) Hydrogenated Polydecene (and) Lauryl Glucoside, Novemer™* EC-2 Polymer (20 %TS)


D. 6. Cetyl Ethylhexanoate, Schercemol™* CO Ester

5.00 Emollient

7. Neopentyl Glycol Dicaprate, Schercemol™* NGDC Ester

5.00 Emollient

8. Aloe Barbadensis Leaf Juice, Aloe Vera 10:1, #01-2113

1.00 Botanical Extract (Skin Conditioner)

9. Fragrance, Wild Orchid / White Tea Fragrance #91-1008-90

0.20 Fragrance

Product Properties: Appearance Opaque lotion

pH 5.5 – 5.7

Viscosity (mPa·s)** 15,000 – 21,000

Stability: Passed 3 months@ 45°C, 4 freeze / thaw cycles. Novemer™* EC-2 Polymer (%TS) 0.80 Recommended Packaging: Qosmedix Airless pump **Brookfield RVT @ 20 rpm, RT, #6 spindle, measured at 24 hours

F-0047



Supplier References: Purac (2)

Lonza (4)

Lubrizol Advanced Materials, Inc. (Noveon®* Consumer Specialties) (5, 6, 7)

Concentrated Aloe Corporation (CAC) (8)

Lebermuth (9)

F-0047

Edition: September 22, 2011

Previous Edition: August 4, 2011

Reference #: 1460-011-10-1 (CSIM) Based on #LLN-002-03-37-MW-040122-1, October 14, 2005

Original Edition: March 17, 2011





TEL: 52.55.3067.0860 FAX: 52.55.5870.8956






TEL: 32.2.678.19.11 FAX: 32.2.678.20.02





Mumbai 400 076 India TEL: 91.22.6698.0590 / 91

FAX: 91.22.6602.7888




Procedure:

1. Combine PART A ingredients. Mix until uniform.

2. Add Glydant® Plus Liquid to batch with mixing. Mix until uniform.

3. Add Novemer™* EC-2 Polymer with mixing. Mix batch until polymer has fully hydrated. Adjust mixing speed as needed to maintain good vortex. Mix until uniform.

4. Add PART D ingredients individually to batch with good mixing in between additions. Mix until uniform.

:

This milky white emulsion is formulated with Pemulen®* TR-1 Polymer as the primary emulsifier. SilSense™* DW-18 Silicone serves to reduce particle size and improve emulsion stability. The overall low level of emulsifier makes this ideal for use on sensitive skin. In addition, the silicone ester helps to improve conditioning and sensory properties of the formulation.

After Shave Balm for Sensitive Skin



2. Glycerin 3.00 Humectant

3. Allantoin 0.10 Soothing Agent

4. Dimethicone PEG-7 Isostearate, SilSense™* DW-18 Silicone

2.00 Particle Size Reducer/ Conditioning Agent

B. 5. Hydrogenated Polydecene, Silkflo® 366 NF

4.00 Emollient

6. Decyl Oleate, Cetiol® V

0.50 Emollient

7. Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Pemulen®* TR-1 Polymer

0.25 Polymeric Emulsifier

C. 8. Diazolidinyl Urea (and) Methylparaben (and) Propylparaben (and) Propylene Glycol, Germaben® II-E

0.80 Preservative

D. 9. Aminomethyl Propanol, AMP-95®

0.18 Neutralizer

E. 10. Fragrance, Portrait

0.50 Perfume

Product Properties: Appearance Milky white emulsion pH 6.3 – 6.7 Viscosity (mPa·s)** 7,200 – 8,000 Stability: Passed 3 months @ 45°C, 5 cycles freeze/thaw ** Brookfield DV – 11+ (or RVT) @ 20 rpm, 25°C, #5 spindle

M-0006

Supplier References: Protameen (2) Lubrizol Advanced Materials, Inc. (Noveon®* Consumer Specialties) (4, 7) Amoco Chemical (5) Cognis (6) ISP (8) Dow (9) Holland Aromatics BV (10)

M-0006 (SIL-0008EU)

Edition: November 2, 2007

Previous Edition: July 8, 2005 Notebook #F0101232

Original Edition: November 6, 2002

Procedure: 1. PART A: Combine ingredients and mix until homogenous.

2. Combine PART B ingredients. Mix to break up any soft lumps of Pemulen®* TR-1 Polymer.

3. Add PART B to PART A. Homogenize with Ultra Turrax for 30 sec.

4. Add PART C to PARTS A and B.

5. Neutralize with PART D under mixing.

6. Add PART E. Stir gently until homogenous.






TEL: 52.55.3067.0860 FAX: 52.55.5870.8956






TEL: 32.2.678.19.11 FAX: 32.2.678.20.02



South Asia 501 Alpha


Mumbai 400 076 India TEL: 91.22.6698.0590 / 91

FAX: 91.22.6698.0599





FormulesFormulesFormules simples & simples & simples & naturellesnaturellesnaturelles

CREAMY EMULSION

1238-2.01




A DEMINERALIZED WATER WATER - - 75,65

AVICEL PC 591 MICROCRYSTALLINE CELLULOSE, CELLULOSE GUM

FMC BIOPOLYMER

gelling agent 2,00

B GLYCERIN GLYCERIN - moisturizing agent

3,00


C EMULIUM

® MELLIFERA

POLYGLYCERYL-6 DISTEARATE,

JOJOBA ESTERS, POLYGLYCERYL-3 BEESWAX, CETYL ALCOHOL


CETEARYL ALCOHOL CETEARYL ALCOHOL - thickening agent

2,00

CETIOL OE DICAPRYLYL ETHER BASF emollient 5,00

JOJOBA OIL SIMMONDSIA CHINENSIS (JOJOBA) SEED OIL

- emollient 3,00

LABRAFACTM

CC CAPRYLIC/CAPRIC TRIGLYCERIDE GATTEFOSSE emollient 5,00


D PERFUME PRECIEUSE 0601579 PARFUM EXPRESSIONS PARFUMEES

perfume 0,15

100,00


- Under rapid mixing (Rotor Stator 2 500 rpm), disperse Avicel PC591 into water for 10min. - Add premix B into A and heat to 75°C. Mix during 10 min. - Under mixing, add C heated to 75°C to A+B heated to 75°C. - Maintain rapid mixing (Rotor Stator 2 500 rpm) for 5-10 min. - Cool under mixing and at about 35°C, add the components of D. - Complete cooling.

Trial Notes

- Aspect : White cream - pH = 6.0+/-0.5 - Viscosity Brookfield RV (spindle B, Speed 5 ) : about 40 000mPa.s after 24H.

NAKED CREAM GEL

1305-1.09




A EMULIUM

® MELLIFERA

POLYGLYCERYL-6 DISTEARATE, JOJOBA ESTERS, POLYGLYCERYL-3 BEESWAX,

CETYL ALCOHOL


MOD OCTYLDODECYL MYRISTATE GATTEFOSSE emollient 10,00



2,00

C HIFORM A 12747 STARCH HYDROXYPROPYL STARCH PHOSPHATE CARGILL gelling agent 2,50

RHEOZAN SH SUCCINOGLYCAN SACI gelling agent 0,50

KONJAC MANNAN GEL POWDER

GLUCOMANNAN SACI gelling agent 0,50

C PRESERVATIVE PRESERVATIVE - preservative 1,00

PERFUME BEAUTY PARFUM FIRMENICH perfume 0,15

100,00


- Under mixing, disperse Hiform A 12747 Starch into water and glycerin of phase B heated to 75°C. - Maintain mixing for about 10 min then under mixing, add Rheozan SH and Konjac Mannan Gel. - Prepare phase A and heat to 75°C. - Under rapid mixing (Rotor/Stator 3000 rpm), add A heated to 75°C to B heated to 75°C. - Maintain rapid mixing for about 10 min. - Cool under mixing and at about 35°C, add the ingredients of phase C. - Complete cooling.

Trial Notes

- Aspect : Bright cream - pH= 6.8 +/- 0.5 - Viscosity Brookfield RV (spindle C, speed 5) : approx. 82 000 mPa.s after 24H.

DELIGHT AND NOURISH

1356-1.11




A EMULIUM

® MELLIFERA

POLYGLYCERYL-6 DISTEARATE, JOJOBA ESTERS, POLYGLYCERYL-3 BEESWAX,

CETYL ALCOHOL


MOD OCTYLDODECYL MYRISTATE GATTEFOSSE emollient 39,0

CETYL ALCOHOL CETYL ALCOHOL - thickening agent

1,5



6,0

AVICEL PC 591 MICROCRYSTALLINE CELLULOSE, CELLULOSE GUM

FMC BIOPOLYMER

gelling agent 1,0


C PERFUME BEAUTY PARFUM FIRMENICH perfume 0,3


100,0


- Prepare B: Heat water to 75°C and under mixing add Avicel PC 591. - Continue mixing for about 15 min. - Add Satiaxane CX 91 under mixing. - Prepare and heat A to 75°C. - Under rapid mixing ( Rotor/Stator 3000rpm), add slowly A heated to 75°C to B heated to 75°C. - Maintain temperature at or below 75°C and mix for about 10 min. - Cool under mixing and at about 35°C, add C. - Complete cooling.

Trial Notes

- Aspect : white thick Lotion - pH= 5.2 +/- 0.5 - Viscosity Brookfield RV (spindle B, speed 5) : approx. 41 000 mPa.s after 24H.

SOOTHING DAY CREAM JB 2730/A





Phase 1EMULIUM ® KAPPA 2 (1) CANDELILLA/JOJOBA/RICE BRAN

POLYGLYCERYL-3 ESTERS (AND) GLYCERYL STEARATE (AND) CETEARYL ALCOHOL (AND) SODIUM STEAROYL LACTYLATE

4.50 O/W emulsifier

CETIOL CC (2) DICAPRYLYL CARBONATE 15.00 EmollientCETYL ALCOHOL (2) CETYL ALCOHOL 2.00 Texture agentPRESERVATIVE 0.80 Preservative

Phase 2DEMINERALIZED WATER WATER 73.10AVICEL PC 591 (3) MICROCRYSTALLINE CELLULOSE

(AND) CELLULOSE GUM2.00 Gelling agent

SATIAXANE CX91 (4) XANTHAN GUM 0.20 Gelling agent

Phase 3GATULINE® DERMA-SENSITIVE (1) OCTYLDODECYL MYRISTATE (AND)

CAPPARIS SPINOSA FRUIT EXTRACT

2.00 Soothing agent

PERFUME VOILE DE DOUCEUR CRE/01629 (5)

0.40 Perfume

100,00(1) GATTEFOSSE SAS / (2) BASF / (3) FMC / (4) CARGILL / (5) MLW

APPAREANCE: Ivory cream

MANUFACTURING PROCESS: - Under mixing, disperse Vivapur Cos 5 then Satiaxane CX 91 into water of phase II heated to 75°C.- Prepare I and heat to 75°C.- Under rapid mixing (rotor/stator 3000 rpm), add I to II, maintain rapid mixing for about 10 min.- Cool under mixing and at about 35°C, add III.- Complete cooling

PROPERTIES: - pH = 5.5 ± 0.5- Viscosity Brookfield (spindle B speed 5) : approx. 40 000 mPa.s after 24H

ASPECT: Crème ivoire

MODE OPERATOIRE: - Sous agitation, disperser le Vivapur Cos 5 puis le Satiaxane CX 91 dans l'eau de II chauffée vers 75°C.- Préparer I et chauffer vers 75°C.- Sous agitation rapide (rotor/stator 3000 tr/min), ajouter I dans II, poursuivre l'agitation rapide pendant 10 min.- Refroidir sous agitation et vers 35°C, ajouter III.- Terminer le refroidissement.

PROPRIÉTÉS: - pH = 5,5 ± 0,5- Viscosité Brookfield (mobile B vitesse 5) : environ 40 000 mPa.s après 24H

FormulesFormulesFormules bébé & enfantbébé & enfantbébé & enfant

EDIBLE MUM AND BABY BALM

1304-1.01




A COMPRITOL® 888 CG GLYCERYL BEHENATE GATTEFOSSE oil gelling agent 5,0

GELEOL GLYCERYL STEARATE GATTEFOSSE thickening agent

5,0

HYDROGENATED CASTOR OIL HYDROGENATED CASTOR OIL - thickening agent 2,5

LIPOCIRETM

A SG C10-18 TRIGLYCERIDES GATTEFOSSE texture agent 10,0

LABRAFAC™ CC CAPRYLIC/CAPRIC TRIGLYCERIDE GATTEFOSSE emollient 72,5

B GLYCERIN GLYCERIN - moisturizing agent

5,0

100,0


- Heat A to 85°C, maintain for 10 min and cool slowly under normal mixing. - At about 45°C increase the mixing speed (rotor/stator 2 500 rpm) - At 35°C add B then mix until completely cooled.

Trial Notes

- Aspect : white thick balm

MOISTURIZING BABY CREAM JB 2806/K

This formula is presented in good faith, however, no warranty as to the accuracy or completeness of results, or fitness for a particular use is given, nor is freedom from the infringement of any intellectual/industrial property rights to be inferred. It is provided "as is" for your consideration, investigation and verification. To the extent permissible by applicable law, Gattefossé shall in no way be liable for any reliance upon information or materials provided.

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Phase Material Name INCI Supplier Properties % Material A PLUROL® STEARIQUE

WL 1009 POLYGLYCERYL-6 DISTEARATE GATTEFOSSE O/W emulsifier 4,00

LIPOCIRE A C10-18 TRIGLYCERIDES GATTEFOSSE emollient feeling agent texture agent

3,00

MOD OCTYLDODECYL MYRISTATE GATTEFOSSE emollient 2,00 CETYL ALCOHOL CETYL ALCOHOL - thickening agent 1,50

ACTICIRE® JOJOBA ESTERS (AND) POLYGLYCERIN-3 (AND) HELIANTHUS ANNUUS SEED CERA (AND) ACACIA DECURRENS FLOWER CERA

GATTEFOSSE moisturizing agent texture agent

1,00

CETIOL OE DICAPRYLYL ETHER BASF emollient 7,00 B DEMINERALIZED

WATER AQUA - 71,00

AVICEL PC 591 MICROCRYSTALLINE CELLULOSE (AND) CELLULOSE GUM

FMC BIOPOLYMER gelling agent 2,00

C GLYCERIN GLYCERIN - moisturizing agent 7,00

SATIAXANE CX91 XANTHAN GUM CARGILL gelling agent 0,20 D PERFUME CAPUCINE

NEW 0610482 PARFUM EXPRESSIONS PARFUMEES perfume 0,30

EUXYL K 712 SODIUM BENZOATE (AND) POTASSIUM SORBATE

SCHULKE & MAYR preservative 1,00

100,00

Operating Instructions - Under mixing, disperse Avicel PC 591 into water of phase B heated to 75°C. - Maintain mixing for about 15 min. - Under mixing, add C to B and maintain mixing for about 5 min more. - Heat phase A to 75°C. - Under rapid mixing ( Rotor/Stator 3000 rpm), add A heated to 75°C to B+C heated to 75°C. - Maintain rapid mixing for about 10 min. - Cool under mixing at about 35°C, add phase D. - Complete cooling.

Trial Notes Aspect: White cream pH = 6.6 ± 0.5 Viscosity Brookfield (spindle C speed 5) : approx. 135 000 mPa.s after 24H

W/O BABY CREAM MM 7516





Phase 1PLUROL® DIISOSTEARIQUE CG (1) POLYGLYCERYL-3 DIISOSTEARATE 6.00 W/O emulsifierHYDROGENATED CASTOR OIL HYDROGENATED CASTOR OIL 1.00 ThickenerWHITE PETROLEUM JELLY P 23 TF (2)

PARAFFINUM LIQUIDUM (AND) CERA MICROCRISTALLINA (AND) PARAFFIN

24.00 Emollient

MOD (1) OCTYLDODECYL MYRISTATE 5.00 EmollientPRESERVATIVE 0.50 Preservative

Phase 2DEMINERALIZED WATER WATER 22.50SODIUM CHLORIDE, CODEX SODIUM CHLORIDE 0.50 StabilizerMAGNESIUM SULFATE 7H2O, CODEX (3)

MAGNESIUM SULFATE 0.50 Stabilizer

Phase 3ZINC OXIDE (4) ZINC OXIDE 40.00 Healing

100,00(1) GATTEFOSSE SAS / (2) AIGLON S.A. / (3) MERCK / (4) COOPERATIVE PHARMAC.FRANCAISE

APPAREANCE: Bright white cream

MANUFACTURING PROCESS: - Under vacuum and rapid stirring (3000 rpm), add II heated to 75°C to I heated to 85°C.- Maintain rapid stirring for 10 min and add Zinc Oxide.- Continue rapid stirring until homogeneous.- Cool under moderate stirring (1500 rd/mn).

PROPERTIES: - Viscosity Brookfield RV (spindle C, speed 5) : approx. 126 000 mPa.s after 24h.

ASPECT: Crème blanche brillante

MODE OPERATOIRE: - Sous vide et sous agitation rapide (3000 tr/min), ajouter II chauffé à 75°C à I chauffé à 85°C.- Maintenir sous agitation rapide pendant 10 mn et ajouter l'Oxyde de Zinc.- Poursuivre l'agitation rapide jusqu'à complète homogénéité.- Refroidir sous agitation modérée (1500tr/mn).

PROPRIÉTÉS: - Viscosité Brookfield RV (mobile C, vitesse 5) : environ 126 000 mPa.s après 24h.

:

This emulsion leaves a smooth, soft feel on the skin and can be applied in a spray form. Pemulen™* TR-2 Polymer stabilizes the suspended tapioca starch. SilSense®* DW-18 Silicone imparts a protective conditioning film and helps Pemulen™* TR-2 Polymer in stabilizing the lotion.

Mommy ’n’ Me Sprayable Liquid Powder



2. Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Pemulen™* TR-2 Polymer

0.15 Polymeric Emulsifier

B. 3. Disodium EDTA, Protacide NA-2

0.05 Chelating Agent

4. Tapioca Starch, Tapioca Pure

10.00 Soothing Agent

C. 5. Isostearyl Isostearate 4.00 Emollient

6. Octyldodecyl Myristate, M.O.D.®

2.00 Emollient

7. Dimethicone PEG-7 Isostearate, SilSense®* DW-18 Silicone

2.00 Conditioner

8. Tocopheryl Acetate, Vitamin E Acetate

0.50 Antioxidant

9. Phenoxyethanol, Methyl-, Ethyl-, Butyl-, Propyl-, and Isobutylparaben, Phenonip®

0.50 Preservative

D. 10. Triethanolamine (99%) 0.20 Neutralizer

E. 11. Fragrance, Floresse BG

0.10 Fragrance

Product Properties: Appearance Thin, white lotion

pH 6.0 – 6.5

Viscosity (mPa·s)** 950 – 1,200

Stability: Passed 3 months @ 45 °C, 5 cycles freeze/thaw ** Brookfield DV - II+ (or RVT) @ 20 rpm, 25°C, # 2 spindle NOTE: Recommended sprayer is supplied by Seaquist Dispersing GmbH, Germany.

• Pump type: PZ2-190 DL with STH • Nozzle type: 4027

Hildebrandstrasse 20, 44319 Dortmund (Wickede) Tel. 02 31 92 40 -0 Fax. 02 31 21 17 52

O-0005(EU)

Supplier References: Lubrizol Advanced Materials, Inc. (Noveon®* Consumer Specialties) (2, 7)

Protameen (3)

National Starch (4)

Gattefossé (6)

BASF (8)

Clariant (9)

Ashland (10)

Holland Aromatics BV (11)

O-0005(EU) (EU-0023)

Edition: 3/16/09

Reference #: F00626.3

Previous Editions: 0-0005 (EU-0023) 9/26/08, 7/8/05

Original Edition: 10/10/01

Procedure: 1. PART A: Disperse Pemulen™* TR-2 Polymer into deionized water at

room temperature.

2. Add PART B ingredients in order to PART A. Mix until homogeneous.

3. In a separate vessel, combine PART C ingredients.

4. Add PART C to PARTS A and B.

5. Homogenize (use Ultra Turrax for 30 seconds) / neutralize with Triethanolamine immediately.

6. Stir slowly. Add PART E.





TEL: 52.55.3067.0860 FAX: 52.55.5870.8956






TEL: 32.2.678.19.11 FAX: 32.2.678.20.02





Mumbai 400 076 India TEL: 91.22.6698.0590 / 91

FAX: 91.22.6602.7888






:

This easy-to-formulate, PEG-Free emulsion is a starting point formula for baby wipes. Glucate™* DO Emulsifier, a vegetable-derived emulsifier, is combined with Pemulen™* TR-2 Polymer and Coco-Glucoside to afford efficient co-stabilization in a simple cold process. Schercemol™* 1818 Ester, also derived from vegetable sources, provides emolliency and a soft afterfeel to this emulsion for gentle, yet effective cleansing wipes.

PEG-Free Emulsion for Baby Wipe (Starting Point Formula)



2. Glycerin 5.00 Humectant

B. 3. Isostearyl Isostearate, Schercemol™* 1818 Ester

2.00 Emollient

4. Bisabolol, (-)Alpha-Bisabolol Natural

0.20 Skin Conditioner

5. Tocopheryl Acetate, Vitamin E Acetate

0.20 Antioxidant

6. Methyl Glucose Dioleate, Glucate™* DO Emulsifier

0.20 Co-Emulsifier

7. Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Pemulen™* TR-2 Polymer


C. 8. Sodium Hydroxide (5%) 0.25 Neutralizer

D. 9. Coco-Glucoside (50%), Plantacare® 818 UP

2.00 Mild Surfactant

E. 10. Phenoxyethanol (and) Ethylhexylglycerin, Euxyl® PE 9010

1.00 Preservative

F. 11. Deionized Water 50.00 Diluent

W-0001(EU)

Product Properties:

Appearance Thin white lotion

pH 5.8 – 6.2

Viscosity (mPa·s)** 400 – 700

Stability: Passed 3 months @ 45 °C and RT,

Passed 5 cycles freeze / thaw ** Brookfield RVT @ 20 rpm, 25°C, #2 spindle, measured after 24 hours

Comments: 1. This formula has not been tested on any non-woven substrate, but is a suggested starting point formulation to help meet difficult viscosity and emulsion stability criteria. Preservation and stability may be dependant on the non-woven substrate that is used for application.

Supplier References: Protameen (2, 5)

Lubrizol Advanced Materials, Inc. (Noveon®* Consumer Specialties) (3, 6, 7)

Symrise (4)

Cognis (9)

Schülke & Mayr (10)

W-0001(EU)

Edition: July 7, 2009

Reference # 081016-04FP, LLN-014-06 (FPC) Original Edition: June 15, 2009





TEL: 52.55.3067.0860 FAX: 52.55.5870.8956






TEL: 32.2.678.19.11 FAX: 32.2.678.20.02





Mumbai 400 076 India TEL: 91.22.6698.0590 / 91

FAX: 91.22.6602.7888






Procedure: 1. PART A: Add Glycerin to Deionized Water.

2. PART B: add ingredients 3-6 in a separate vessel. Disperse Pemulen™* TR-2 Polymer into oil phase.

3. Add PART B to PART A. Mix for 20-30 minutes to allow the polymer to swell.

4. Neutralize batch with Sodium Hydroxide (5%). Mix vigorously until uniform.

5. Add Coco-Glucoside. Mix slowly to avoid air entrapment.

6. Add preservative (ingredient #10). Mix until uniform.

7. Dilute with Deionized Water. Mix until uniform.

Soins Soins Soins spécifiquesspécifiquesspécifiques

CLOUD MASK

JB 2840/H

This formula is presented in good faith, however, no warranty as to the accuracy or completeness of results, or fitness for a particular use is given, nor is freedom from the infringement of any intellectual/industrial property rights to be inferred. It is provided "as is" for your consideration, investigation and verification. To the extent permissible by applicable law, Gattefossé shall in no way be liable for any reliance upon information or materials provided.

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A DEMINERALIZED WATER WATER - 84,80

MAKIMOUSSE 25 SODIUM POLYACRYLATE STARCH DAITO KASEI texture agent 0,50

B EMULIUM® DELTA

CETYL ALCOHOL (AND) GLYCERYL STEARATE (AND) PEG-75 STEARATE (AND) CETETH-20 (AND) STEARETH-20


LABRAFAC CC CAPRYLIC/CAPRIC TRIGLYCERIDE GATTEFOSSE emollient 10,00

PHYLDERM® VEGETAL C2 HYDROLYZED SOY PROTEIN GATTEFOSSE

energizing agent nourishing agent

1,50

C PERFUME LIN ET COTON PARFUM - perfume 0,20

PHENOXYETHANOL PHENOXYETHANOL - preservative 0,90

ETHYLHEXYLGLYCERIN ETHYLHEXYLGLYCERIN - preservative 0,10

100,00


- Under rapid mixing, add Makimousse 25 to water of phase A heated to 75°C, maintain rapid mixing for about 10 min. - Heat phase B to 75°C. - Under rapid mixing (Rotor/Stator 3000 rpm), add B to A. - Maintain rapid mixing for about 10 min. - Cool under mixing and at about 35°C, add the ingredients of phase C. - Complete cooling.

Trial Notes

- Aspect: Foamy cream - pH = 7.0 ± 0.5 - Viscosity Brookfield (spindle C speed 5) : approx. 72 000 mPa.s after 24H

This toner is ideal to be used after the skin is washed and before using other cosmetic preparations. It tones and relaxes the skin with its refreshing, moisturizing and nourishing properties. Pemulen™* TR-2 polymeric emulsifier offers excellent stability to this low viscosity milky toner with 6% emollient esters. The distinct emulsification property of Pemulen™* TR-2 polymeric emulsifier contributes to the watery refreshing burst as the toner is being applied on the skin and also offers a non-tacky, low-residue afterfeel. The combination of Schercemol™* NGDO, SHS, 318 and DISD esters, offers a cascading emolliency which leaves the skin with a cushiony, smooth feel. This combination of esters also aids skin hydration and prevents skin dryness by replenishing the lipids that are removed by frequent washing.

Translucent Skin Toner

INCI Name, Trade Name Weight % Function A. 1. Isostearyl Hydroxystearate,

Schercemol™* SHS Ester 0.75 Emollient

2. Diisostearyl Dimer Dilinoleate, Schercemol™* DISD Ester

0.75 Emollient

3. Isopropyl Isostearate, Schercemol™* 318 Ester

1.50 Emollient

4. Neopentyl Glycol Diethylhexanoate, Schercemol™* NGDO Ester

3.00 Emollient

B. 5. Acrylates/C10-30 Alkyl Acrylate Crosspolymer, Pemulen™* TR-2 Polymeric Emulsifier

0.12 Emulsifier

C. 6. Deionized Water 93.66 Diluent

7. Disodium EDTA 0.04 Chelating Agent

D. 8. Sodium Hydroxide (18%) 0.12 Neutralizer

E. 9. Methylisothiazolinone (and) Ethylhexylglycerin (and) Water, Euxyl® K 220

0.06 Preservative

Product Properties: Appearance Milky liquid, applies translucent pH 5.5 – 6.5 Viscosity (mPa·s)** 400 – 900 Stability: Passed 3 months @ 25 & 45°C, Passed 5 freeze/thaw cycles Polymer (%TS) 0.12 ** Brookfield RVT Viscometer spindle #2 @ 30 rpm, @ 60 s

O-0050B(AP)

Supplier References: Lubrizol Advanced Materials, Inc. (1, 2, 3, 4, 5) Schülke & Mayr GmbH (9)

O-0050B(AP)

Based on O-0050(AP)

Edition: March 13, 2012 Previous Editions: 2/15/2012, 1/5/2012

Reference #: SG1469-001-11-005 (POMA)

Original Edition: December 16, 2011 O-0050(AP):Original Reference #: SG1469-001-11-

009(POMA) O-0050 Original Edition: October 14, 2011

Procedure: 1. PART A: Add all the ingredients to the main vessel, heat to 48~52°C with

gentle mixing. 2. Disperse Pemulen™* TR-2 polymeric emulsifier in PART A. Mix until

uniform with no lumps maintaining temperature of 48~52°C. 3. PART C: In a side vessel, dissolve Disodium EDTA in the solution of

Deionized Water with mixing @ 45~50°C. 4. Add PART C to main batch with mixing, maintaining temperature of 48~52°C.

Mix until uniform. 5. Mix batch at high speed for 10 minutes, while maintaining temperature of

48~52°C. 6. Cool batch to 40°C with mixing. 7. Neutralize batch with Sodium Hydroxide (18%) with high speed mixing. Mix

until uniform. 8. Decrease mixing speed and continue cooling to 35°C. 9. Add ingredient 9 to batch with mixing. Mix until uniform.

Lubrizol Advanced Materials, Inc. / 9911 Brecksville Road, Cleveland, Ohio 44141-3247 / TEL: 800.379.5389 or 216.447.5000 The information contained herein is being furnished for

informational purposes only, upon the express condition that the User makes its own assessment of the appropriate use of such information. While the information contained herein is believed to be reliable, no representations, guarantees or warranties of any kind are made as to its accuracy, suitability for a particular application or the results to be obtained herefrom. Lubrizol Advanced Materials, Inc. ("Lubrizol") cannot guarantee how any products associated with this information will perform

in combination with other substances or in User’s process. Due to the variations in methods, conditions and equipment used commercially in processing these materials, no warranties or guarantees are made as to the suitability of the information/products for the applications disclosed. Lubrizol shall not be liable and the User assumes all risk and responsibility for, any use or handling of any material beyond Lubrizol's direct control. LUBRIZOL MAKES NO WARRANTIES, EXPRESS OR IMPLIED, INCLUDING, BUT NOT

LIMITED TO, THE IMPLIED WARRANTIES OF MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE. It is the User’s sole responsibility to determine if there are any issues relating to patent infringement of any component or combination of components relating to the supplied information. Nothing contained herein is to be considered as permission, recommendation, nor as an inducement to practice any patented invention without the permission of the patent owner.

For further information, please visit: www.lubrizol.com/personalcare Lubrizol Advanced Materials, Inc. is a wholly owned subsidiary of The Lubrizol Corporation

*Trademark owned by The Lubrizol Corporation © Copyright 2012 / The Lubrizol Corporation

http://www.lubrizol.com/personalcare

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